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Title:
EFFECT OF 1-HEXANOL CO-SURFACTANT ON THE NiFe NANOPARTICLES DENSITY IN REVERSE MICROEMULSION SYSTEMS

Authors:
Mayda Lam Maldonado, Jose Aaron Melo Banda, David Macias Ferrer

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Mayda Lam Maldonado, Jose Aaron Melo Banda, David Macias Ferrer
Centro de Investigacion en Petroquimica Secundaria, Instituto Tecnologico de Cd. Madero, Cd. Madero, Tamaulipas, 89440, Mexico

MLA 8
Maldonado, Mayda L., et al. "EFFECT OF 1-HEXANOL CO-SURFACTANT ON THE NiFe NANOPARTICLES DENSITY IN REVERSE MICROEMULSION SYSTEMS." IJETSI, vol. 3, no. 1, pp. 63-68, ijetsi.org/more2018.php?id=5.
APA
Maldonado, M. L., Banda, J. M., & Ferrer, D. M. (n.d.). EFFECT OF 1-HEXANOL CO-SURFACTANT ON THE NiFe NANOPARTICLES DENSITY IN REVERSE MICROEMULSION SYSTEMS. IJETSI, 3(1), 63-68. Retrieved from http://ijetsi.org/more2018.php?id=5
Chicago
Maldonado, Mayda L., Jose Aaron M. Banda, and David M. Ferrer. "EFFECT OF 1-HEXANOL CO-SURFACTANT ON THE NiFe NANOPARTICLES DENSITY IN REVERSE MICROEMULSION SYSTEMS." IJETSI 3, no. 1 (n.d.), 63-68. http://ijetsi.org/more2018.php?id=5.

References
[1]. Khadzhiev S.N., Kadiev K.M., Yampolskaya G.P. and Kadieva M.K., "Trends in the Synthesis of Metal Oxide Nanoparticles Through Reverse Microemulsions in Hydrocarbon Media", Adv. Colloid Interface Sci., Vol. 197, pp. 132-145, 2013
[2]. Zuev Yu.F., Mirgorodskaya A.B., Kudryavtseva L.A., Idiyatullin B.Z. and Khamidullin R.N., "Influence of the Structure of Cetyltrimethylammonium Bromide Based Microemulsions on Base Hydrolysis of Carboxylic Acid Esters", Russian Journal of General Chemistry, Vol. 74(7), pp. 1051-1056, 2004
[3]. El-Laithy H.M., "Preparation and Physicochemical Characterization of Dioctyl Sodium Sulfosuccinate (Aerosol OT) Microemulsion for Oral Drug Delivery", AAPS PharmSciTech., Vol. 41(1), pp. 80-89, 2003
[4]. Verhoeckx G.J., De Bruyn P.L. and Overbeek J.Th.G., "On Understanding Microemulsions", J. Colloid Interface Sci., Vol. 119(2), 409-421, 1987
[5]. Caboi F., Capuzzi G., Baglioni P. and Monduzzi M., "Microstructure of Ca-AOT/Water/Decane w/o Microemulsions", J. Phys. Chem. B, Vol. 101(49), pp.10205-10212, 1997
[6]. Arvidsson A. and Soderman O., "The Microemulsion Phase in the Didecyldimethylammonium Bromide / Dodecane / Water System. Phase Diagram, Micro-structure, and Nucleation Kinetics of Excess Oil Phase", Langmuir, Vol. 17(12), pp. 3567-3572, 2001
[7] . Choi S.Y., Oh S.G., Bae S.Y. and Moon S.K., "Effect of Short-Chain Alcohols as Co-Surfactants on Pseudo-Ternary Phase Diagrams Containing Lecithin", Korean J. Chem. Eng., Vol. 16(3), pp. 377-381, 1999
[8]. Tadros Tharwat F., "Applied Surfactants: Principles and Applications." WILEY-VCH Verlag GmbH & Co.KGaA, 2005
[9] . Hossain S., Fatema U.K., Y.A. Mollah, Rahman M. and Susan A.B.H., "Microemulsions as Nanoreactors for Preparation of Nanoparticles with Antibacterial Activity", J. Bangladesh Chem. Soc., Vol. 25(1), pp. 71-79, 2012
[10]. Wongwailikhit K. and Horwongsakul S., "The Preparation of Iron (III) Oxide Nanoparticles using W/O Microemulsion", Mater. Letters, Vol. 65(17- 18), pp. 2820-2822, 2011
[11]. Liu C. and Zhang Z.J., "SizeDependent Super-paramagnetic Properties of Mn Spinel Ferrite Nanoparticles Synthesized from Reverse Micelles", Chem. Mater., Vol. 13, pp. 2092-2096, 2001
[12]. Han D.Y., Yang H.Y., Shen C.B. Zhou X. and Wang F.H., "Synthesis and size control of NiO nanoparticles by water-in-oil microemulsion", Powder Technol., Vol. 147, pp. 113-116, 2004
[13]. Lopez-Quintela M.A., Tojo C., Blanco M.C., Garcia Rio L. and Leis J.R., "Microemulsion Dynamics and Reactions in Microemulsions" Current Opinion in Colloid Interface Sci., Vol. 9, pp. 264-278, 2004
[14]. Malik M.A., Wani M.Y., Hashim M.A., "Micro-emulsion method: A novel route to synthesize organic and inorganic nanomaterials" Arabian J. Chem., Vol. 5, pp. 397-417, 2012

Abstract:
In this work, NiFe nanoparticles with molar ratio (1:1) have been synthesized through inverse microemulsion method using water, sodium dodecylbenzenesulfonate as surfactant, toluene as continuous phase, sodium borohydride as reductant agent and citric acid as stabilizing agent, studying the effect on the density of NiFe nanoparticles by the addition of co-surfactant 1- hexanol, thus NiFe (1:1)-A (without 1-hexanol) and NiFe (1:1)-B (with 1-hexanol) were analyzed. The NiFe microemulsion systems was characterized by means atomic absorption (AA), dynamic light scattering (DLS), scanning transmission electron microscopy (STEM) and energy-dispersive x-ray spectroscopy (EDS). The effect of the co-surfactant showed greater stability in the microemulsion, obtaining a higher density of NiFe nanoparticles in comparison with the microemulsion without 1-hexanol. In both microemulsions, nanoparticles with spherical morphology with diameters less than 20 nm were obtained.

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